The Transforminator was developed by Specialized Formulations to upgrade their customers Mk IIIA Terpenators to use a larger base, so as to allow the use of larger columns.
It is basically a 6" X 10" or 12" end cap reducer, and the appropriately sized tank to match.
They added 45 degree bend in the recovery leg for more clearance and a sight glass on that leg to watch for liquid aspiration.
As far as operating instructions, If you can run a Mk III, you know how to run them all.
I would personally also upgrade to the Mk IV bi-directional flood design, which you can the details of at http://skunkpharmresearch.com/the-mk-iva-phoenix-terpenator/
WolfWurx's Mk IVB Terpenator bi-directional flooding Operating Instructions as follows:
1.0 Starting up a dormant system:
1.1 Visually and tactically inspect system for:
1.1.1 Loose clamps, or clamps that are not uniformly tensioned.
1.1.1.1 Viton gasket clamp bolts are torqued to 44 inch pounds.
1.1.1.2 PTFE gasket clamp bolts are torqued to 50 inch pounds.
1.1.2 Any clamped joint misalignment suggesting potential sealing issues.
1.1.3 Loose hoses or compression fittings.
1.1.4 Loose filter drier cartridges.
1.1.5 Any staining at connections, suggesting low level leaks on previous runs.
1.2 Evacuate the system.
1.2.1 Using the attached Mk IV-B PID drawing, all valves are opened except back fill valve 9, the refrigerant tank valves 18 and 19, as well as valve 14, the vacuum pump isolation valve, and valve 25, the nitrogen valve.
1.2.2 Start high vacuum pump 8, and when running smoothly, open valve 14.
1.2.3 Evacuate the atmosphere from the system to a level of 30" (29.92") Hg on the analog gauge.
1.2.4 When 30" Hg is achieved, close the vacuum pump isolation valve 14.
1.2.5 Shut off vacuum pump.
1.2.6 Allow to soak for 5 minutes and monitor pressure using compound pressure gauge 9, to detect any rise in pressure, indicating a leak.
1.2.7 If vacuum decay is detected, remediate source of leak until vacuum levels hold steady for 5 minutes.
1.3 Inject refrigerant:
1.3.1 Start room ventilation:
1.3.2 Close butane injection valves 6 and 13.
1.3.3 Open tank valves 18 and 19.
1.3.4 Open valve 6 for 10 seconds and then close.
1.4 Inspect for leaks:
1.4.1 Using a portable Hydrocarbon Detector, inspect for leaks at all Triclamp connections.
1.4.2 Check all hose connections, especially valves 4, 6, 18, 19, and 24.
1.4.3 Inspect for leaks at valves 4, 6, 11, 13, 14, 15, 17, 18, and 19, both at the NPT fitting, and at the valve stem.
1.4.4 Check for leaks in the column head assembly threaded joints at 3, 4, 5, and 6.
1.4.5 Remediate any leaks and retest until leak free.
1.5 Recover refrigerant:
1.5.1 Start pneumatic recovery pump 2, by opening valve 1.
1.5.2 Recover to -22" Hg.
1.5.3 Close valve 11.
1.5.4 Turn off recovery pump 2, by closing valve 1 and 11.
1.5.3 Inject nitrogen until zero pressure gauge is reached using valve .
1.5.4 Start vacuum pump.
1.5.5 Open valve 14 once vacuum pump has smoothed out.
1.5.6 Evacuate to -29.9" Hg.
2.0 Operating the Mk IVB Terpenator
2.1 Load the prepared material into the column:
2.1.1 Remove the column from the Mk IVB using a 5/8" wrench to remove the 2 clamp bolts.
2.1.2 Inspect the column and seals for cleanliness and clean as required using denatured alcohol.
2.1.3 Clamp a blank end cap on one of the column, using a hinged speed clamp, and pack wadded commercial coffee filters in the bottom firmly, using a 2" or larger dowel.
2.1.4 Pack the material firmly and evenly every six inches or so, until the column is loaded within an inch of the end.
2.1.5 Finish the column by packing two more wadded coffee filters in the last inch, and set aside for mounting on the machine.
2.2 Mounting the columns.
2.2.1 Place a screened gasket on top the Mk IV injection manifold, and set the open column end on the gasket, centering it using the raised ridge on the sanitary seals.
2.2.2 Install the two bolt high pressure clamp, and tighten uniformly.
2.2.3 Remove the clamp and end cap from the other end of the column, and after setting a screened gasket in place, place the column head on top and center it on the sanitary seal ridge.
2.2.4 Install the two bolt high pressure clamp and tighten uniformly.
2.2.5 Check the tightness of all clamps and hose connections.
2.3 Preparing system:
2.3.1 Turn on ancillaries:
2.3.1.1 Turn on chamber ventilation.
2.3.1.2 If using water heat, turn on pot circulation pump 21, using switch 25, and verify flow by observing discharge in hot pot 22.
2.3.1.3 Observe water temperature on PID controller for process specified.
2.3.1.3.1 85F for carboxylic acid
2.3.1.3.2 200F for maximum speed extracting essential oils to subsequently be decarboxylated for topical or oral use.
2.3.1.4 If using silicone mat heaters, turn on power to the lower pot heater, but not the column heaters, at controller 20.
2.3.1.5 Add ice and water to ice bath 23.
2.3.1.5.1 May also add dry ice, depending on process.
2.4 Evacuating the system.
2.4.1 Using the attached Mk IV-B PID drawing, all valves are opened except the backfill valve 9, the refrigerant tank valve 18, as well as valve 14, the vacuum pump isolation valve, and valve 25, the nitrogen backfill valve.
2.4.2 Start high vacuum pump 8, and when running smoothly, open valve 14.
2.4.3 Evacuate the atmosphere from the system to a level of 30" (29.92") Hg on the analog gauge, to exclude oxygen from the system.
2.4.4 When 30" Hg is achieved, close the vacuum pump isolation valve 14.
2.4.5 Shut off vacuum pump.
2.4.6 Allow to soak for 5 minutes and monitor pressure using compound pressure gauge 9, to detect any rise in pressure, indicating a leak.
2.4.7 If vacuum decay is detected, remediate source of leak until vacuum levels hold steady for 5 minutes.
2.4.8 Once vacuum stability is achieved for 5 minutes, close dump valve 17, and column recovery valve 15.
2.4.8.1 Close butane flood valves 6 and 13.
2.4.8.2 Open solvent tank storage tank valves 18 and 19.
2.5 Safety checking the system.
2.5.1 Listen for leaks in the line from the Haskel pump 2 and the tank connection valve 19, as well as the line from the refrigerant tank to the Terpenator injection valves.
2.5.2 Using a Hydrocarbon Leak Detector, check for leaks in the liquid butane line from points 18, to points 6 and 13.
2.5.2.1 Check for hose leaks by sight and sound.
2.5.2.2 Check at locations 6,13, 18, and 24 specifically.
2.6 Flood the system.
2.6.1 Start recovery pump 2, by opening valve 1.
2.6.2 To flood, open valve 13 and time how long it takes until the liquid flows through sight glass 5.
5.2.1 Record that time.
2.6.3 Continue to flood for the additional specified period of time , or until the color of the oil passing through sight glass 5 clears.
2.6.4 Close vent valve 4.
2.6.5 Close flood valve 13.
2.6.6 Slowly open valve 17, so as to not splash when the column dumps.
2.6.7 Open rinse valve 6 for the specified period of time.
2.6.8 Close rinse valve 6.
2.7 Recover to -10" Hg
2.7.1 Allow recovery pump to lower system pressure to -10" Hg, and then close valve 17.
2.8 Repeat for as many cycles as required to fully extract the material being processed.
2.9 Finish process:
2.9.1 When last cycle reaches -10" Hg, close dump valve 17 and open column recovery valve 15, to recover the column separately from the lower pot.
2.9.2 Turn on column heat.
2.9.2.1 If hot water heat, turn on Circulation pump 32 using switch 33.
2.9.2.2 If heat mats, turn on controller at control 20.
2.9.3 Continue to pump until -22" Hg is reached.
2.9.4 Turn off valve 11.
2.9.5 Turn off valve 1
2.9.6 Turn on valve 25 and inject nitrogen until zero pressure is reached.
2.9.6.1 Nitrogen regulator pressure not to exceed 50 psi.
2.9.6.2 Turn off valve 25 at zero gauge.
2.9.7 Turn on switch 7 to start vacuum pump.
2.9.8 When pump smooths out, open vacuum pump isolation valve 14.
2.9.9 Evacuate to -29.9" Hg.
2.9.10 Hold at high vacuum for length of time specified on process.
2.9.10.1 Repeat 2.9.6 through 2.9.9" Hg if excessive pressure rise is noted during soak.
3.0 Harvesting the extracted essential oils and oleoresins:
3.1 Open vent 9 to equalize pressure.
3.2 Remove 2 bolt high pressure clamp 30 from the 10" lid on lower recovery tank 29.
3.3 Remove lid assembly and clean underside using 190 proof ethanol. Set aside alcohol mixture.
3.4 Set lid assembly on clean lower tank bottom and replace clamp 30.
3.5 Return Mk IVB to service.
3.6 Two methods of harvesting the extracted oleoresins.
3.6.1 Place lower tank in 0F freezer for 30 minutes before scraping out of tank using PTFE scraper.
3.6.1.1 Further process as required for end use.
3.6.2 Wash out with 190 proof ethanol.
3.6.2.1 Place in 0F freezer for 48 hours to winterize.
3.6.2.2 Filter at 15 microns to remove precipitated waxes.
3.6.2.3 Remove alcohol using Rotovape and vacuum oven.
That pic does not help me my friend!!
Thanks Gw for the instructions!! Can the mk3 6" collection chamber be used to make the transforminator without adding the bigger chamber. I am only using a 12" x 1.5" column and wondering if it is worth to make it into the transforminator? Thanks
Thanks Gw for the instructions!! Can the mk3 6" collection chamber be used to make the transforminator without adding the bigger chamber. I am only using a 12" x 1.5" column and wondering if it is worth to make it into the transforminator? Thanks
I don't care if people think I am being a dick because I don't hold their hand when there is tons of information available if you read, I don't want someone to blow themselves up because they can't take a few hours to educate themselves.
A person just spends a few grand on equipment and doesn't learn how to use it? I don't get it, sorry.
Im not opposed to asking a question, but hand holding someone through working a big potentially explosive device is in my opinion not something that should be done... unless its in a classroom setting
Could GW list operating instructions for the mk3 bi directional flow extractor.From can tapping to doing an extraction? Thanks again GW
See I was going to say that but im already giving 707 franchise a hard time with this and I dont want to be the house dbag, mostly because theres enough here already. Nssknight, Flatslabs is totally right man, dont risk hurting yourself or someone else because you dont take the time to learn. Knowledge is power brother