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Terpenation at Terpene Station

icdog

Member
I'm trying to find a filter drier, looked for the parker 303 or ek032/084. I don't really have a clue what it is so its not easy to source in Canada, no surprise!
Is there anything specific I need to know to find one, those brands might not be available here so does it need to do something certain to work?
 

Gray Wolf

A Posse ad Esse. From Possibility to realization.
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Bluebery

New member
The refrigeration pump I have is a Amprobe promax Rg5000. The phone number and address is from the east coast. There's an online owners manual and it seems to be rated for everything the Appion is. Maybe there's a spec I'm spacing about. Read something about cleaning an Appion with butane and charcoal i think that sparked my curiosity. Thanks
 

nakadashi

Member
The refrigeration pump I have is a Amprobe promax Rg5000. The phone number and address is from the east coast. There's an online owners manual and it seems to be rated for everything the Appion is. Maybe there's a spec I'm spacing about. Read something about cleaning an Appion with butane and charcoal i think that sparked my curiosity. Thanks
I think what u might be referring to is maintainence on the recovery pump if you suspect BHO got in, u can do this by running liquid butane through the pump and letting it shoot into the air.

Regarding using charcoal, it is a process to filter out undesirable stuff from canned butane by loading activated carbon into the system and running the liquid butane through it.
 

nakadashi

Member
Just did my first dry ice run today with no heat on the collection chamber today, got the lightest shatter ever! I tried Mr. Durden's technique of leaving about an inch of butane and pouring it off... very convenient but I definitely need more practice to get it down.

I am completely sold on dry ice now. For the first time I was able to totally burp the tank. I waited till the top of the tank was reading -4 and left the vapor port open until no more gas came out. It was a loooooooooong wait. I guess this whole time I have been running the system with a lot of other gases besides butane! I remember GW correctly recommending burping out gases in the storage tank as the solution to another user's long recovery times, so I was expecting faster recovery times as well. On the contrary everything went slower. The initial flood took over 30 seconds! I was not sure what was going on but I saw ice creeping up the column so I knew the sub-zero butane was slowly but surely making its way up.

Now I am of the opinion that that the CPS Pro-Set MT69 is mandatory with dry ice. I noticed that the top of the butane storage tank became warmer through the course of one run (from -4F up to 30F), even though I have it loaded in a cooler with 25 lb of dry ice. Also the liquid butane coming from the storage tank got warmer and warmer as I progressed further into the run. I suspect the submersible cooler will help in keeping the butane in the storage tank much cooler. Are you guys experiencing the same thing with dry ice?
 

nakadashi

Member
Right now I'm using a 5 CU Ft chest freezer with a 30# bottle in an anti-freeze bath, teflon core stainless steel braid covered hoses and a MT69 CPS Molecular Transformator Recovery Submersible Subcooler in its own anti-freeze bath. Cost me pennies to run the freezer and dry ice is spendy and over an hour away from my lab.

What are the temps like with this setup? (temps of butane entering the system, and temps of the antifreeze bath?) I am not too keen on constantly refilling on dry ice as it is $1.25/lb here and I suspect my cooler may not have stellar insulation.
 

Gray Wolf

A Posse ad Esse. From Possibility to realization.
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ICMag Donor
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Just did my first dry ice run today with no heat on the collection chamber today, got the lightest shatter ever! I tried Mr. Durden's technique of leaving about an inch of butane and pouring it off... very convenient but I definitely need more practice to get it down.

I am completely sold on dry ice now. For the first time I was able to totally burp the tank. I waited till the top of the tank was reading -4 and left the vapor port open until no more gas came out. It was a loooooooooong wait. I guess this whole time I have been running the system with a lot of other gases besides butane! I remember GW correctly recommending burping out gases in the storage tank as the solution to another user's long recovery times, so I was expecting faster recovery times as well. On the contrary everything went slower. The initial flood took over 30 seconds! I was not sure what was going on but I saw ice creeping up the column so I knew the sub-zero butane was slowly but surely making its way up.

Now I am of the opinion that that the CPS Pro-Set MT69 is mandatory with dry ice. I noticed that the top of the butane storage tank became warmer through the course of one run (from -4F up to 30F), even though I have it loaded in a cooler with 25 lb of dry ice. Also the liquid butane coming from the storage tank got warmer and warmer as I progressed further into the run. I suspect the submersible cooler will help in keeping the butane in the storage tank much cooler. Are you guys experiencing the same thing with dry ice?

At -4F, you still have propane pressure, which helps speed up the floods. I just burp off the air, and leave the propane.
 
Just did my first dry ice run today with no heat on the collection chamber today, got the lightest shatter ever! I tried Mr. Durden's technique of leaving about an inch of butane and pouring it off... very convenient but I definitely need more practice to get it down.

I am completely sold on dry ice now. For the first time I was able to totally burp the tank. I waited till the top of the tank was reading -4 and left the vapor port open until no more gas came out. It was a loooooooooong wait. I guess this whole time I have been running the system with a lot of other gases besides butane! I remember GW correctly recommending burping out gases in the storage tank as the solution to another user's long recovery times, so I was expecting faster recovery times as well. On the contrary everything went slower. The initial flood took over 30 seconds! I was not sure what was going on but I saw ice creeping up the column so I knew the sub-zero butane was slowly but surely making its way up.

Now I am of the opinion that that the CPS Pro-Set MT69 is mandatory with dry ice. I noticed that the top of the butane storage tank became warmer through the course of one run (from -4F up to 30F), even though I have it loaded in a cooler with 25 lb of dry ice. Also the liquid butane coming from the storage tank got warmer and warmer as I progressed further into the run. I suspect the submersible cooler will help in keeping the butane in the storage tank much cooler. Are you guys experiencing the same thing with dry ice?

Glad you are liking the cold method :) you can do it with just ice too. When using dry ice, don't run more than two tubes. It gets so cold you'll get clumping of paraffin wax and recovery times are slow :-\ just in case, keep a fine mesh strainer handy.

Scrape up all the wax stuck at the bottom and sides and use it to make an absolute. There will be some oil content in it

I wouldn't even bother burping your tank, especially with ďry ice, as you lose all your pressure which results in long runs till it is built back up. Or just burp for twenty seconds or less

Just add more butane to build it back up if need be.

Not sure the mt69 is mandatory, but it is nice :) just run it with ice though. I freeze tupperware with water in it for that, as ice is cheap, and no need to waste dry ice on cooling that warm butane. With the mt69 , the hose leaving it is very cold versus the one leaving the appion

Sent from my GT-N7100 using Tapatalk now Free
 
1/4" JIC and 1/4 SAE are interchangeable and should work fine on 1/4 refrigerant hoses. However once you go to 3/8, you must have a JIC fitting on both or SAE on both. The difference between SAE and JIC is the angle of the flare. Flexicraft also sells the JIC flare fittings, which are stainless, which i prefer over brass. All stainless terp ftw

I went with 1/4" male npt and then added yellow jacket 19129. sure you'll have to replace the gasket once in awhile, but i'm just not sure if that metal to metal connection is designed for being taken on and off on a daily basis. of course i need to look into this still
 
What are the temps like with this setup? (temps of butane entering the system, and temps of the antifreeze bath?) I am not too keen on constantly refilling on dry ice as it is $1.25/lb here and I suspect my cooler may not have stellar insulation.

try setting up an account with your local dry ice outfit. It cut my cost in half. they don't ask what it is for and you don't need a business license or anything, although i do. not that they asked to see it. just fill out the credit form but tell them you just want to do COD
 
At -4F, you still have propane pressure, which helps speed up the floods. I just burp off the air, and leave the propane.

i think it is hard to determine where the air ends and the propane or butane starts.... at least it was for me. :/

hey GW, do you have any pics posted of your Ia with the 3x36 tube being used? i'm curious how it is stacked as I'd like to build one.

is it 1" ball valve, 1x3 concentric reducer/ filler tube, 3x36" tube, concentric reducer 3x1.5", sight glass, end cap to 1/4" female npt?
 
It is usually dry already and we tend to collect it for awhile before mixing with alcohol. In the end, it ends up in the same place

Sent from my GT-N7100 using Tapatalk now Free
 
I'm trying to find a filter drier, looked for the parker 303 or ek032/084. I don't really have a clue what it is so its not easy to source in Canada, no surprise!
Is there anything specific I need to know to find one, those brands might not be available here so does it need to do something certain to work?

Just go big on the filter. They are called filter dryers. Just use eBay. I have a sight glass ahead of mine so my filter has 1/4 males on both ends

Sent from my GT-N7100 using Tapatalk now Free
 

nakadashi

Member
i think it is hard to determine where the air ends and the propane or butane starts.... at least it was for me. :/
Yes very difficult. I kept wondering when I was supposed to smell something sweet. I guess I just don't find propane sweet because soon it was all gone!
 
Yes very difficult. I kept wondering when I was supposed to smell something sweet. I guess I just don't find propane sweet because soon it was all gone!

yeah, always smelled like butane to me. i just weighed it while doing so to make sure i wasn't losing an insane amount of butane. in the end i stopped burping. not necessary with dry ice.
 
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