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#21
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From your link: 2. Will the chemicals involved in your application be effectively filtered with the available carbon filters? Protector Airo Filtered Fume Hood is a ductless fume hood that uses Neutrodine Filters.Typically, ductless hoods will be outfitted with chemical specific filters. Specific filter types increase chemical trapping capacity for different chemical families; however, some chemicals cannot be safely filtered or aren’t filtered effectively enough to allow ductless hoods to be a financially viable option. Filtered fume hoods can filter out acids, bases, and solvents with one filter type, however, there are still some chemicals (low molecular weight solvents) that will not be effectively filtered. ...some organics (such as methanol) are very volatile, light weight, and are not effectively adsorbed on the organic filter. There are a large number of videos on commercial and DIY design, construction, and testing of fume hoods at YouTube.
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Link won't open? 1. Click on the link. 2. Click in the address bar, and use backspace to remove the s in https. 3. Click on the 'reload this page' icon, or hit the return key. Best to Worst Canned Butane List https://www.icmag.com/ic/showpost.ph...6&postcount=28 Cannabis Alchemy by D. Gold https://calgarycmmc.com/E-books/E%20B...0D.%20Gold.pdf Hash oil techniques and solvents for non BHO hash oil? https://www.icmag.com/ic/showthread.php?t=338633 Solvents listed as to polarity https://www.icmag.com/ic/showpost.ph...&postcount=162 The Truth Machine by James L. Halperin (free read provided by the author) https://coins.ha.com/information/ttm.s |
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#22
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There are a number of components on Ebay that may be useful (if you're an eBay type person).
I had not considered a benchtop unit but at $200 to $300, I saw a number of quick answers. There seemed to be several of these for sale... https://www.ebay.com/itm/Labconco-39...AAAOSwmkpZ6rZ9 |
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#23
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Thanks for all the details! I am curious, is it standard operating procedure for labs (professional of all sort across industries) to just dump fume hood exhaust into the atmosphere? If I understand correctly, the tall stack mixes in fresh air to lower the concentration of compounds, but they are still getting expelled. Is it ethical to release methanol (for instance) vapor if people and/or pets could be in the area outside? Or are concentrations so low as not to matter?
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#24
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Examples of local exhaust ventilation - https://www.bwc.ohio.gov/downloads/b...3-1-5-99.2.pdf |
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#25
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Whatever the authorities allow. It would take a lot of butane to challenge any decent 8" inline to explode, as long as the fan was on first.
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In the clinical field, the practical application of these substances must be awaited with the usual necessary patience. - Roger Adams Marihuana February 19, 1942 |
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#26
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Those were taken from Industrial Ventilation. Imagine the whole book.
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An age is called Dark not because the light fails to shine, but because people refuse to see it. Believing is seeing and ignorance is bliss until it bites you in the ass! Fervor is the weapon of the impotent. The harder the sell, the poorer the product. Alas, my ignorance abounds; the more I've learned, the less I know that I know.......... Thou shalt seek and respect the opinions of operators, even unto the third helper, for theirs is a wisdom unknown to technicrats. Wise men learn more from fools, than fools from wise men. In my dotage I finally discovered that the secret to putting on pants both legs at a time is sitting down. |
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#27
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A company's discharge permit spells out how many tons of VOC's they are dumping per year and what it is. A single cabinet would be a small source, and DEQ is after the big polluters, so unless someone is complaining about the smell, or you set something on fire, it is unlikely they will show up. Dumping it high in the air and mixing the discharge using an evase is a dilution solution to smell and concentration. For safety, the fumes going through a non explosion proof fan should be below Lower Explosive Limits, which is relatively low for alcohol and the alkanes. 1.2% for hexane, 1.4% pentane, 1.8% butane, 2.1 % Propane, 2.2% Iso, and 3.3% ethanol. With an explosion proof fan an evase will help dilute the discharge below explosive limits. We used an explosion proof confined space inline ventilator fan, readily available at your corner safety equipment store. https://www.industrialfansdirect.com...ns-and-blowers
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An age is called Dark not because the light fails to shine, but because people refuse to see it. Believing is seeing and ignorance is bliss until it bites you in the ass! Fervor is the weapon of the impotent. The harder the sell, the poorer the product. Alas, my ignorance abounds; the more I've learned, the less I know that I know.......... Thou shalt seek and respect the opinions of operators, even unto the third helper, for theirs is a wisdom unknown to technicrats. Wise men learn more from fools, than fools from wise men. In my dotage I finally discovered that the secret to putting on pants both legs at a time is sitting down. |
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#28
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Thanks guys. I really need to think the exhaust path through. Will read more and post back soon.
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#29
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In industry, all engineering avenues must be exhausted, before relying on personal protection, or challenging standards. When dealing with OSHA, the engineering values that you must meet, are taken from Ventilation Handbook. They of course have averages and safety factors, and you can design below that and sometimes still be effective, but they are actually pretty accurate and while you can sometimes get away with values below them, you can't defend your position if it doesn't work. I come from an industry, where OSHA is constantly at your door protecting us'n, so suggest considering all designs from that perspective. If challenged, is it defensible by the accepted authority and the numbers?? There is of course the really keen and significant up side to such a resource as Industrial Ventilation, which is that the governmental hygienist writing it, actually did know what they were doing and it does work, as judged from a professional lifetime of practical experience applying their principles.
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An age is called Dark not because the light fails to shine, but because people refuse to see it. Believing is seeing and ignorance is bliss until it bites you in the ass! Fervor is the weapon of the impotent. The harder the sell, the poorer the product. Alas, my ignorance abounds; the more I've learned, the less I know that I know.......... Thou shalt seek and respect the opinions of operators, even unto the third helper, for theirs is a wisdom unknown to technicrats. Wise men learn more from fools, than fools from wise men. In my dotage I finally discovered that the secret to putting on pants both legs at a time is sitting down. Last edited by Gray Wolf; 03-28-2018 at 08:04 PM.. |
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#30
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I don't have a fume hood yet.
I do make sure my window is always open when I play with chemicals. As long as my vapors get diluted by fresh outdoor air I think my chances of problems are greatly reduced. I won't do chemical reactions without fresh air and I prefer when the temperature is less than 15C outside. Cold air makes for easier distillations and solvent reclamation.
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