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Old 02-12-2018, 12:24 PM #11
Gray Wolf
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Quote:
Originally Posted by Noperuiy View Post
As the title said . This is my first run of fractional distill . I used the oil which run from rotovap vap first to seperate alcohol . Then i run it through fractional distill . The result come out quite clear and light yellow but it ... stink ? Any one experience with this problem ?
Your help is much appreciate !
Sounds like you didn't distill off all the first fraction before switching.
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Old 02-12-2018, 04:04 PM #12
Noperuiy
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@ gray wolf : thanks a lot ! That what i think too . I will leave it a bit longer before changing the flask !
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