|
in:
|
|
| Forums > Talk About It! > Cannabis Concentrates > Operator Closed Loop Water Error | ||
Post Reply  |
| Operator Closed Loop Water Error | Thread Tools | Search this Thread |
11-13-2017, 07:42 PM
|
#1 |
|
Member
Join Date: Jan 2010
Posts: 149
 |
Operator Closed Loop Water Error
One of my trained staff somehow ended up with water in the end product (locked within a valve or another means) after a 48 hour purge it still pops on the nail test not due to solvent since a side by side slab was ran back to back and it is proper but by this water.
In the past I throw it into a column with the same strain and re run it and getting back basically double what I normally yield pour on 2 trays etc and turns out just fine. This time it was the last of the strain any thoughts on to getting that moisture out? Was thinking throw it into 2 reducer cones connected to each other and running cold solvent over the frozen cones but any other ideas are welcome Thanks!
__________________
"When you smoke the herb it reveals you to yourself" - Bob Marley 
|
|
|
|
11-13-2017, 07:58 PM
|
#2 |
|
Seed Whore
Join Date: Dec 2016
Location: In the Fridge
Posts: 1,603
 |
Maybe get a desiccator?
Desiccators are sometimes used to remove traces of water from an almost-dry sample. https://en.wikipedia.org/wiki/Desiccator
__________________
I just died. |
|
|
|
|
11-13-2017, 08:11 PM
|
#3 |
|
Member
Join Date: Jan 2010
Posts: 149
|
I have a heated one available and also an oven just didnt want to crank temps and lose alot of the goodies in the process
__________________
"When you smoke the herb it reveals you to yourself" - Bob Marley
|
|
|
|
|
11-13-2017, 09:01 PM
|
#4 |
|
A Posse ad Esse. From Possibility to realization.
  
Join Date: Apr 2009
Location: River City, USA
Posts: 9,402
|
What temperature and vacuum level are you purging at?
__________________
An age is called Dark not because the light fails to shine, but because people refuse to see it. Believing is seeing and ignorance is bliss until it bites you in the ass! Fervor is the weapon of the impotent. The harder the sell, the poorer the product. Alas, my ignorance abounds; the more I've learned, the less I know that I know.......... Thou shalt seek and respect the opinions of operators, even unto the third helper, for theirs is a wisdom unknown to technicrats. Wise men learn more from fools, than fools from wise men. In my dotage I finally discovered that the secret to putting on pants both legs at a time is sitting down. |
|
|
|
|
11-13-2017, 09:41 PM
|
#5 |
|
Member
Join Date: Jan 2010
Posts: 149
|
97 degrees and 28.5 in hg because of the elevation Im located in.
__________________
"When you smoke the herb it reveals you to yourself" - Bob Marley
|
|
|
|
|
11-13-2017, 11:54 PM
|
#6 | |
|
A Posse ad Esse. From Possibility to realization.
Join Date: Apr 2009
Location: River City, USA
Posts: 9,402
|
Quote:
|
|
|
|
|
|
11-14-2017, 08:27 AM
|
#7 |
|
Member
Join Date: Jan 2010
Posts: 149
|
will do definitely before having to re process. Will get the last slabs out and try a 115 purge to get the moisture out. Slab will most likely be "sugaring" up by that time
__________________
"When you smoke the herb it reveals you to yourself" - Bob Marley
|
|
|
1 members found this post helpful. |
| Post Reply |
«
Previous Thread
|
Next Thread
»
|
|
All times are GMT +2. The time now is 02:35 PM.
