einsteinlady
Member
I'll soak hemp in n-hexane
Filter through vacuumed Buchner with activated charcoal
Rotovap under vacuum (water aspirated vacuum pump)until hexanes recovered
Add ethanol to oil to wash it and rotovap that mostly off
Purge in vac oven
What do you think? Any tips?
What temperature should I keep water bath while while rotovaping the hexane off while under vacuum?
Safety is top priority. I plan on soaking hemp with hexane outside and after filtering pour it into 5 liter evaporating flask and bring inside where rotovap will be. Should I rotovap outside? or would I need an explosion proof fan exhausting room too.
Filter through vacuumed Buchner with activated charcoal
Rotovap under vacuum (water aspirated vacuum pump)until hexanes recovered
Add ethanol to oil to wash it and rotovap that mostly off
Purge in vac oven
What do you think? Any tips?
What temperature should I keep water bath while while rotovaping the hexane off while under vacuum?
Safety is top priority. I plan on soaking hemp with hexane outside and after filtering pour it into 5 liter evaporating flask and bring inside where rotovap will be. Should I rotovap outside? or would I need an explosion proof fan exhausting room too.