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Showing results 1 to 50 of 173
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Posts Made By:
thegreenman91
Forum:
Cannabis Concentrates
08-17-2017, 04:28 PM
Replies:
23
Rotovap vs SprayVap
Views:
3,833
Posted By
thegreenman91
What kind of space do you have yours set up in?...
What kind of space do you have yours set up in? Does this thing create a lot of heat?
Forum:
Cannabis Concentrates
08-04-2017, 01:33 AM
Replies:
7
Winterization Black crystal form at completion
Views:
818
Posted By
thegreenman91
Try lye/water mixture. thats worked wonders for...
Try lye/water mixture. thats worked wonders for my glass.
Forum:
Cannabis Concentrates
08-03-2017, 06:38 PM
Replies:
7
Winterization Black crystal form at completion
Views:
818
Posted By
thegreenman91
We're running it up to 110c at the end to decarb...
We're running it up to 110c at the end to decarb and then hitting 120c just to pour. The solids fall out between the 100c-110c mark.
Forum:
Cannabis Concentrates
08-03-2017, 04:02 AM
Replies:
3
Precipitate Forming During QWET runs
Views:
434
Posted By
thegreenman91
Hi I am curious if you found a solution to this...
Hi I am curious if you found a solution to this problem. Also what type of ethanol are you using: corn, wheat, sugar?
Forum:
Cannabis Concentrates
08-02-2017, 09:31 PM
Replies:
7
Winterization Black crystal form at completion
Views:
818
Posted By
thegreenman91
We're using a 20l AI rotovap
We're using a 20l AI rotovap
Forum:
Cannabis Concentrates
08-01-2017, 08:31 PM
Replies:
7
Winterization Black crystal form at completion
Views:
818
Posted By
thegreenman91
I have been having this same issue on ethanol...
I have been having this same issue on ethanol extractions of plant material (not winterized bho). My idea was that ultrafine plant material was strong through the fritter disc, switched to a table...
Forum:
Cannabis Concentrates
05-17-2017, 06:24 AM
Replies:
7
CO2 super fractionation
Views:
1,672
Posted By
thegreenman91
The waters machine fractionates into 3 vessles
The waters machine fractionates into 3 vessles
Forum:
Cannabis Concentrates
03-10-2017, 07:30 PM
Replies:
267
The Clear .............Thread!
Views:
39,994
Posted By
thegreenman91
I have gotten distillate that shatters as well. I...
I have gotten distillate that shatters as well. I find that like with coconut oil which at one temperature is solid and hard but a couple of degrees higher is completely liquid and runny, when...
Forum:
Cannabis Concentrates
10-31-2016, 05:45 PM
Replies:
31
Thca crystalline
Views:
8,133
Posted By
thegreenman91
It still seems to me that it would be quite...
It still seems to me that it would be quite difficult for a company to pump out large amounts of thc-a crystals through simple evaporative crystallization. I think acid/base extraction MUST be...
Forum:
Cannabis Concentrates
10-07-2016, 11:30 PM
Replies:
8
Issues with Potency
Views:
801
Posted By
thegreenman91
Absolutely, I understand 100%.... even on a...
Absolutely, I understand 100%.... even on a second pass the potency is coming back a few percentage points lower than the first.
Also, it's not like the yield after distillation was better than...
Forum:
Cannabis Concentrates
10-07-2016, 10:16 PM
Replies:
8
Issues with Potency
Views:
801
Posted By
thegreenman91
Issues with Potency
This is a quick and simple question for all you people...
I've had many batches of non-winterized distillate coming out after a single pass at easily over 80% THC.... sometimes peaking at about...
Forum:
Cannabis Concentrates
09-04-2016, 09:11 PM
Replies:
8
BHO-RSO-BUTTER
Views:
522
Posted By
thegreenman91
If your going for a food grade oil, and you're...
If your going for a food grade oil, and you're making rosin why not just squish the living hell out of your buds at a relatively warm temperature to extract everything you can. Collect the oil,...
Forum:
Cannabis Concentrates
09-04-2016, 09:06 PM
Replies:
5
Turning cow receiver under high vacuum
Views:
544
Posted By
thegreenman91
I couldn't imagine stopping the vacuum every time...
I couldn't imagine stopping the vacuum every time you need to change fractions. Any time I have had to stop a vac during a run I've had a bad time after the fact, in my experience stopping the vac...
Forum:
Cannabis Concentrates
08-22-2016, 11:52 PM
Replies:
22
Rso vs bho
Views:
2,513
Posted By
thegreenman91
On the topic of sugars.... and other essential...
On the topic of sugars.... and other essential plant nutrients. How does this apply to growth practices. Say for example someone were to load their plant up with sugars (mollasses or other...
Forum:
Cannabis Concentrates
08-11-2016, 09:55 PM
Replies:
19
lipid not settling to the bottom during winterization?
Views:
1,978
Posted By
thegreenman91
Hey Grey Wolf... Is there a good centrifuge for...
Hey Grey Wolf... Is there a good centrifuge for our industry? The largest I can find is 6x 1000ml. Is there a centrifuge with a large sized single bucket design that could effectively be used for...
Forum:
Cannabis Concentrates
08-10-2016, 04:38 PM
Replies:
4
Who's eating thc-a? What effects are you experiencing?
Views:
488
Posted By
thegreenman91
Most people are smoking it. Seems like a waste to...
Most people are smoking it. Seems like a waste to me.
Forum:
Cannabis Concentrates
08-09-2016, 11:31 PM
Replies:
209
Preparation of crystalline THCA
Views:
106,667
Posted By
thegreenman91
Thanks for the explanation!
Thanks for the explanation!
Forum:
Cannabis Concentrates
08-08-2016, 10:46 PM
Replies:
209
Preparation of crystalline THCA
Views:
106,667
Posted By
thegreenman91
This is what I want to know.
This is what I want to know.
Forum:
Cannabis Concentrates
08-06-2016, 10:25 PM
Replies:
103
Isolating Cannabis Terpenes, Part II: Actual Process
Views:
14,771
Posted By
thegreenman91
How's this workin out for you lately Phenome?
How's this workin out for you lately Phenome?
Forum:
Cannabis Concentrates
07-24-2016, 09:52 PM
Replies:
10
High volume Buchner
Views:
1,616
Posted By
thegreenman91
What would you say is quicker? Vacuum filtration...
What would you say is quicker? Vacuum filtration or pressurized?
Forum:
Cannabis Concentrates
07-13-2016, 10:23 PM
Replies:
17
Relationship between stability and quality
Views:
1,252
Posted By
thegreenman91
I think we need to make a distinction here...
I think we need to make a distinction here between "stability" and "hardness". Chemical stability is a completely different story than the hardness or dryness of wax or shatter.
When talking...
Forum:
Cannabis Concentrates
07-13-2016, 09:55 PM
Replies:
492
Short Path Distillation
Views:
106,096
Posted By
thegreenman91
check out https://www.vacuu-lan.com/ they do whole...
check out https://www.vacuu-lan.com/ they do whole lab vacuum systems but I am sure you could imagine up your own and order parts through them.
Forum:
Cannabis Concentrates
07-05-2016, 06:13 PM
Replies:
9
How long do you cure before blasting?
Views:
757
Posted By
thegreenman91
Awesome charts PDX, any chance you have a link to...
Awesome charts PDX, any chance you have a link to the study?
Forum:
Cannabis Concentrates
07-04-2016, 06:27 PM
Replies:
15
Dabbers...Let's have a discussion...
Views:
1,783
Posted By
thegreenman91
I like stainless steel lab spatulas best. However...
I like stainless steel lab spatulas best. However most of the time I use tools out of a 12 piece clay carving set. Or a regular titanium carbcap/dabber. I dislike those however because the rounded...
Forum:
Cannabis Concentrates
07-02-2016, 03:29 AM
Replies:
492
Short Path Distillation
Views:
106,096
Posted By
thegreenman91
Usually at the end of the run I leave the boiling...
Usually at the end of the run I leave the boiling flask to cool overnight, warm it back up in the morning, pour out the residue and immediately pour in ISO, swish it around and the iso it heats up....
Forum:
Cannabis Concentrates
06-28-2016, 11:08 PM
Replies:
492
Short Path Distillation
Views:
106,096
Posted By
thegreenman91
What do you mean when you say water gets sucked...
What do you mean when you say water gets sucked in through the joints.
Running co2 extracted material (high water content) I have seen air leaking through the ground glass joint on the boiling...
Forum:
Cannabis Concentrates
06-28-2016, 05:12 PM
Replies:
492
Short Path Distillation
Views:
106,096
Posted By
thegreenman91
@oldgold Are you working with hydrocarbon...
@oldgold Are you working with hydrocarbon extracted or co2 extracted material?
Forum:
Cannabis Concentrates
06-27-2016, 09:32 AM
Replies:
19
What has more flavor? Live resin or 'fresh' bubble hash?
Views:
2,638
Posted By
thegreenman91
Live resin. I find that non solvent extracted...
Live resin. I find that non solvent extracted concentrates almost always have a sort of charred flavor that is hard to describe but personally it is noticeable enough for me to make that distinction....
Forum:
Cannabis Concentrates
06-12-2016, 09:50 AM
Replies:
6
Bho yields
Views:
1,466
Posted By
thegreenman91
This is something I have been thinking about....
This is something I have been thinking about. Current thoughts are that, as you said, THC-A decarboxilates readily under low heat. Then how is it that purified/crystallized THC-A does not self...
Forum:
Cannabis Botany and Advanced Growing Science
06-08-2016, 05:21 PM
Replies:
12
Double veg not reveg anyone ever try?
Views:
877
Posted By
thegreenman91
Sounds not entirely unlike flowering a mother...
Sounds not entirely unlike flowering a mother plant.
Forum:
Cannabis Concentrates
06-07-2016, 05:50 AM
Replies:
53
extraction under 98.6* F
Views:
6,261
Posted By
thegreenman91
Are you huffing diethyl ether?
Are you huffing diethyl ether?
Forum:
Cannabis Concentrates
06-07-2016, 12:00 AM
Replies:
53
extraction under 98.6* F
Views:
6,261
Posted By
thegreenman91
Something tells me this guys extract has his...
Something tells me this guys extract has his brain a little scrambled up.
Forum:
Cannabis Concentrates
06-03-2016, 06:40 PM
Replies:
26
Removing THC from CBD concentrate - Help !!!
Views:
5,464
Posted By
thegreenman91
I think you should be more concerned with...
I think you should be more concerned with purifying that crude paste before worrying about removing the THC. What is the other 80% of your extract?
Forum:
Cannabis Concentrates
05-21-2016, 02:40 AM
Replies:
149
Isolation of THCA
Views:
35,662
Posted By
thegreenman91
AND also.... Shouldnt 99.997% THC-A...
AND also.... Shouldnt 99.997% THC-A (guildextracts) decarboxilate at room temperature?
Forum:
Cannabis Concentrates
05-12-2016, 10:19 PM
Replies:
12
Cloudy patches on my crystal clear shatter
Views:
1,241
Posted By
thegreenman91
water
water
Forum:
Cannabis Concentrates
05-05-2016, 05:10 AM
Replies:
103
Isolating Cannabis Terpenes, Part II: Actual Process
Views:
14,771
Posted By
thegreenman91
I looked into this as well... all I could find...
I looked into this as well... all I could find through the Blue River website was a link for patent information to their corporate website. Here all I saw was patent pending on their Prana line.
Forum:
Cannabis Concentrates
05-05-2016, 12:40 AM
Replies:
103
Isolating Cannabis Terpenes, Part II: Actual Process
Views:
14,771
Posted By
thegreenman91
Fuckin nice job!
Fuckin nice job!
Forum:
Cannabis Concentrates
05-03-2016, 09:55 AM
Replies:
15
Decarb under vacuum?
Views:
2,157
Posted By
thegreenman91
I let it go overnight on 1500-2000 gram batches...
I let it go overnight on 1500-2000 gram batches at 120c. Works out to complete decarb plus a bit extra. Works for the company but of I was creating my own medicine I would do different.
Forum:
Cannabis Concentrates
05-03-2016, 12:21 AM
Replies:
54
Shatter, wax, crumble?
Views:
35,343
Posted By
thegreenman91
Superior, yes. But definitely not...
Superior, yes. But definitely not "healthier"
Forum:
Cannabis Concentrates
05-03-2016, 12:01 AM
Replies:
492
Short Path Distillation
Views:
106,096
Posted By
thegreenman91
Oil darkens. Temp drops slightly then starts to...
Oil darkens. Temp drops slightly then starts to spike. It's entirely up to you when to stop the process and pull your fraction.
Forum:
Cannabis Concentrates
05-02-2016, 11:54 PM
Replies:
15
Decarb under vacuum?
Views:
2,157
Posted By
thegreenman91
But that's not to say that decarbinv until you...
But that's not to say that decarbinv until you get some cbn is not worth it. I like it when I get some decarbed oil with 2-4% cbn for the night. Use that in the morning and it's a day ruiner
Forum:
Cannabis Concentrates
05-02-2016, 11:49 PM
Replies:
16
Winterizing into shatter? Help!
Views:
1,436
Posted By
thegreenman91
I would never put boiling butane in a sealed box...
I would never put boiling butane in a sealed box chilled with electric motors.
Forum:
Cannabis Concentrates
04-29-2016, 09:05 PM
Replies:
15
Decarb under vacuum?
Views:
2,157
Posted By
thegreenman91
You are correct. I feel like alot of the fear of...
You are correct. I feel like alot of the fear of turning product to CBN comes from the same side that thinks cured bud is decarbed. Test results will tell you.
Forum:
Cannabis Concentrates
04-28-2016, 04:49 PM
Replies:
15
Decarb under vacuum?
Views:
2,157
Posted By
thegreenman91
I decarb under partial vac in a rotovap, helps...
I decarb under partial vac in a rotovap, helps pull water out of co2 oil as well and protect the oil from oxidation.
Forum:
Cannabis Concentrates
04-27-2016, 10:32 PM
Replies:
30
The quest for shattery shatter
Views:
1,951
Posted By
thegreenman91
Super simple stuff!
Super simple stuff!
Forum:
Cannabis Concentrates
04-26-2016, 02:18 AM
Replies:
492
Short Path Distillation
Views:
106,096
Posted By
thegreenman91
https://www.popeinc.com/uploads/files/literature/Wi...
https://www.popeinc.com/uploads/files/literature/Wiped_Film.pdf
20" diameter column. This is where the industry is headed with tech.
Forum:
Cannabis Concentrates
04-22-2016, 04:55 PM
Replies:
492
Short Path Distillation
Views:
106,096
Posted By
thegreenman91
That's a pretty quick change of opinion there. If...
That's a pretty quick change of opinion there. If it doesn't taste like limonene how did he remove it to such levels?
Forum:
Cannabis Concentrates
04-22-2016, 03:30 AM
Replies:
492
Short Path Distillation
Views:
106,096
Posted By
thegreenman91
I guess spending 12 hours a day in your lab...
I guess spending 12 hours a day in your lab distilling limonene kinda kills your perception of it eh?
Forum:
Cannabis Concentrates
04-21-2016, 06:33 PM
Replies:
492
Short Path Distillation
Views:
106,096
Posted By
thegreenman91
You are always very confident that any LHO will...
You are always very confident that any LHO will still smell like oranges. What do you think about people claiming they can get it down to below sensory threshold?
Forum:
Cannabis Concentrates
04-19-2016, 05:04 PM
Replies:
30
The quest for shattery shatter
Views:
1,951
Posted By
thegreenman91
Low enough temps to avoid decarboxilization. ...
Low enough temps to avoid decarboxilization.
High enough temps (enough drying of volatile terpenes) to deplete the terpene content to increase hardness without decarbing
4 things cause...
Showing results 1 to 50 of 173
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